MICROEXTRACTION BY DEMIXING FOR THE DETERMINATION OF VOLATILE COMPOUNDS IN AQUEOUS-SOLUTIONS

被引:37
作者
CACHO, J
FERREIRA, V
FERNANDEZ, P
机构
[1] Department of Analytical Chemistry, Faculty of Science, University of Zaragoza
关键词
GAS CHROMATOGRAPHY; DEMIXING; EXTRACTION; VOLATILE COMPOUNDS;
D O I
10.1016/0003-2670(92)87020-L
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A method for the determination of volatile compounds present in aqueous solutions is presented, based on microextraction by demixing with 2-propanol. The extraction properties of various solvents were examined and the method was optimized. The method is rapid and precise and enables detection limits of 1-mu-g l-1 to be attained with flame ionization detection using only one concentration step.
引用
收藏
页码:311 / 317
页数:7
相关论文
共 5 条
[1]   SPECTROPHOTOMETRIC DETERMINATION OF TOTAL MONOTERPENOLS AT LOW CONCENTRATIONS [J].
CACHO, J ;
FERREIRA, V .
ANALYST, 1990, 115 (05) :657-661
[2]   ON-COLUMN INJECTION OF LARGE SAMPLE VOLUMES USING THE RETENTION GAP TECHNIQUE IN CAPILLARY GAS-CHROMATOGRAPHY [J].
GROB, K ;
KARRER, G ;
RIEKKOLA, ML .
JOURNAL OF CHROMATOGRAPHY, 1985, 334 (02) :129-155
[3]   SAMPLE RECONCENTRATION BY COLUMN-EXTERNAL SOLVENT EVAPORATION OR INJECTION OF LARGE VOLUMES INTO GAS-CHROMATOGRAPHIC CAPILLARY COLUMNS [J].
GROB, K ;
MULLER, E .
JOURNAL OF CHROMATOGRAPHY, 1987, 404 (02) :297-305
[4]   ORGANIC-SUBSTANCES IN POTABLE WATER AND IN ITS PRECURSOR .3. CLOSED-LOOP STRIPPING PROCEDURE COMPARED WITH RAPID LIQUID EXTRACTION [J].
GROB, K ;
GROB, K ;
GROB, G .
JOURNAL OF CHROMATOGRAPHY, 1975, 106 (02) :299-315
[5]  
Jennings W., 1981, FLAVOUR 81, P233