N-VINYL AS N-H PROTECTING GROUP - CONVENIENT SYNTHESIS OF MYOSMINE

被引：41

作者：

BRANDANGE, S ^{[1
]}

LINDBLOM, L ^{[1
]}

机构：

[1] UNIV STOCKHOLM, DEPT ORG CHEM, ARRHENIUS LAB, S-10405 STOCKHOLM, SWEDEN

来源：

ACTA CHEMICA SCANDINAVICA SERIES B-ORGANIC CHEMISTRY AND BIOCHEMISTRY | 1976年 / 30卷 / 01期

关键词：

D O I：

10.3891/acta.chem.scand.30b-0093

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

N-vinylpyrrolidone was condensed with nicotinate. The condensation product was treated with boiling concentrated HCl. After extraction of bases and distillation, myosmine, a tobacco alkaloid, was obtained in a 63% yield.

引用

页码：93 / 93

页数：1

共 3 条

[1] BETA-DICARBONYLVERBINDUNGEN ALS AMINOSCHUTZGRUPPEN BEI PEPTIDSYNTHESEN [J].

DANE, E ;

DOCKNER, T ;

DREES, F ;

KONRAD, P .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1962, 74 (21) :873-&

[2] CHEMICAL STUDIES ON TOBACCO-SMOKE .23. SYNTHESIS OF C-14-LABELED MYOSMINE, NORNICOTINE AND N'-NITROSONORNICOTINE [J].

HU, MW ;

BONDINEL.WE ;

HOFFMANN, D .

JOURNAL OF LABELLED COMPOUNDS, 1974, 10 (01) :79-88

[3] ACYL-LACTON-UMLAGERUNG .22. UMLAGERUNG VON ALPHA-AROYL-PYRROLIDONEN IN KONZ. SALZSAURE ZU PYRROLINDERIVATEN [J].

KORTE, F ;

SCHULZES.HJ .

CHEMISCHE BERICHTE-RECUEIL, 1962, 95 (10) :2444-&

← 1 →