Mapping the elemental distribution in sol-gel derived ceramics

被引：4

作者：

Houk, CS ^{[1
]}

Page, CJ ^{[1
]}

机构：

[1] UNIV OREGON,DEPT CHEM,EUGENE,OR 97403

来源：

ADVANCED MATERIALS | 1996年 / 8卷 / 02期

关键词：

D O I：

10.1002/adma.19960080218

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Elemental dispersive X-ray (EDX) composition distribution mapping using a scanning electronmicroscope (SEM) provides information about samples that is complementary to that obtained from X-ray diffraction. Examples are given (e.g., Ba and Cu maps of YBa2CU3O7-delta see figure) to demonstrate the usefulness of this technique in evaluating the homogeneity of sol-gel products and in elucidating elemental zoning (see also cover picture).

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页码：173 / &

页数：5

相关论文

共 16 条

[1] COMPOSITION CONTROL OF THE MICROSTRUCTURE OF BA2YCU3O6+X [J].

BLENDELL, JE ;

HANDWERKER, CA ;

VAUDIN, MD ;

FULLER, ER .

JOURNAL OF CRYSTAL GROWTH, 1988, 89 (01) :93-100

[2] MICRO-ANALYSIS BY A FLYING-SPOT X-RAY METHOD [J].

COSSLETT, VE ;

DUNCUMB, P .

NATURE, 1956, 177 (4521) :1172-1173

[3]

GOLDSTEIN JI, 1992, SCANNING ELECT MICRO, P525

[4] APPLICATION OF ENERGY-DISPERSIVE X-RAY ELEMENTAL MAPPING TO PROBE THE HOMOGENEITY OF SOL-GEL DERIVED YBA2CU3O7-DELTA AND RELATED PHASES [J].

HOUK, CS ;

BURGOINE, GA ;

PAGE, CJ .

CHEMISTRY OF MATERIALS, 1995, 7 (04) :649-656

[5]

LAUNEAU P, 1994, CAN MINERAL, V32, P919

[6] SOL-GEL PROCESSING OF TRANSITION-METAL ALKOXIDES FOR ELECTRONICS [J].

LEE, GR ;

CRAYSTON, JA .

ADVANCED MATERIALS, 1993, 5 (06) :434-442

[7] SOL-GEL CHEMISTRY OF TRANSITION-METAL OXIDES [J].

LIVAGE, J ;

HENRY, M ;

SANCHEZ, C .

PROGRESS IN SOLID STATE CHEMISTRY, 1988, 18 (04) :259-341

[8] SUBSTRATE FILM INTERACTIONS IN THICK-FILMS OF YBACUO ON ALUMINA [J].

MADHAVRAO, L ;

RAJAGOPALAN, R .

JOURNAL OF MATERIALS SCIENCE, 1990, 25 (05) :2349-2352

[9]

MARINENKO RB, 1991, MICROBEAM ANAL, P333

[10] EVALUATION OF A POTENTIAL DENTAL APPLICATION OF VAPOR-DEPOSITION TECHNIQUES FOR COATING ALUMINA WITH TIN OXIDE [J].

MCCRORY, PV ;

PIDDOCK, V ;

COMBE, EC ;

TINSTON, S ;

ARNELL, RD ;

WEGLICKI, P ;

OWEN, J .

JOURNAL OF MATERIALS SCIENCE-MATERIALS IN MEDICINE, 1994, 5 (08) :543-550