NOVEL FRAGMENTATION OF TRIMETHYLSILYL ETHERS OF 3BETA-HYDROXY-DELTA-5-STEROIDS

被引：19

作者：

BJORKHEM, I ^{[1
]}

GUSTAFSS.JA ^{[1
]}

SJOVALL, J ^{[1
]}

机构：

[1] KAROLINSKA INST,KEM INST,STOCKHOLM 60,SWEDEN

来源：

ORGANIC MASS SPECTROMETRY | 1973年 / 7卷 / 03期

关键词：

D O I：

10.1002/oms.1210070305

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

引用

页码：277 / 281

页数：5

共 13 条

[1] SYNTHESIS OF 3BETA-HYDROXY-DELTA5-STEROIDS BY SODIUM BORO-HYDRIDE REDUCTION OF DIENOL TRIMETHYLSILYL ETHER DERIVATIVES OF 3-OXO-DELTA4-STEROIDS [J].

ARINGER, L ;

ENEROTH, P .

STEROIDS, 1971, 18 (04) :381-&

[2] METABOLISM OF STEROIDS IN GERMFREE AND CONVENTIONAL RATS TREATED WITH A 3BETA-HYDROXY-DELTA5-STEROID OXIDOREDUCTASE INHIBITOR [J].

BJORKHEM, I ;

GUSTAFSS.JA ;

GUSTAFSS.SA .

EUROPEAN JOURNAL OF BIOCHEMISTRY, 1970, 16 (03) :557-&

[3] METABOLISM OF 3BETA-HYDROXY-DELTA5- AND 3-OXO-DELTA4-C-19 AND C21 STEROIDS IN HUMAN LIVER-MICROSOMES [J].

BJORKHEM, I ;

SOMELL, A ;

EINARSSON, K ;

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ACTA ENDOCRINOLOGICA, 1972, 71 (03) :569-+

[4] MASS SPECTROMETRY IN STRUCTURAL AND STEREOCHEMICAL PROBLEMS .125. MASS SPECTROMETRY OF SOME STEROID TRIMETHYLSILYL ETHERS [J].

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DJERASSI, C .

JOURNAL OF ORGANIC CHEMISTRY, 1967, 32 (04) :1005-&

[5] IDENTIFICATION OF 22-HYDROXYCHOLESTEROL 24-HYDROXYCHOLESTEROL AND 26-HYDROXYCHOLESTEROL IN STEROID SULPHATE FRACTION OF FAECES FROM INFANTS [J].

GUSTAFSSON, JA ;

SJOVALL, J .

EUROPEAN JOURNAL OF BIOCHEMISTRY, 1969, 8 (04) :467-+

[6] DATA ACQUISTION AND EVALUATING SYSTEMS FOR A LOW RESOLUTION MASS SPECTROMETER [J].

HEDFJALL, B ;

JANSSON, PA ;

MARDE, Y ;

RYHAGE, R ;

WIKSTROM, S .

JOURNAL OF PHYSICS E-SCIENTIFIC INSTRUMENTS, 1969, 2 (12) :1031-&

[7] OXIDATION OF CHOLESTEROL, 3BETA-HYDROXY-5-PREGNEN-20-ONE AND 3BETA-HYDROXY-5-ANDROSTEN-17-ONE BY RAT LIVER MICROSOMES [J].

JOHANSSON, G .

EUROPEAN JOURNAL OF BIOCHEMISTRY, 1971, 21 (01) :68-+

[8] MASS SPECTROMETRY IN STRUCTURAL AND STEREOCHEMICAL PROBLEMS CLI . FURTHER STUDIES ON MASS SPECTROMETRY OF 17-KETO STEROIDS [J].

JONES, G ;

DJERASSI, C .

STEROIDS, 1967, 10 (06) :653-&

[9] OXYGEN-18 EXCHANGE REACTIONS IN STEROIDAL KETONES . DETERMINATION OF RELATIVE RATES OF INCORPORATION BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY [J].

LAWSON, AM ;

LEEMANS, FAJ ;

MCCLOSKEY, JA .

STEROIDS, 1969, 14 (05) :603-+

[10] ANALYSIS OF STEROIDS BY OFF-LINE COMPUTERIZED GAS CHROMATOGRAPHY MASS SPECTROMETRY [J].

REIMENDAL, R ;

SJOVALL, J .

ANALYTICAL CHEMISTRY, 1972, 44 (01) :21-+

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